Thermo stimulated creep analysis is performed to characterize the anelastic properties in the glassy state of the epoxy resin-glass bead model system. Different interphase regions have been deliberately formed by means of a silane coupling agent and an elastomeric adduct coating. By applying 'fractional stresses', with a convenient choice of the loading programme, the complex/3 peak is experimentally resolved and local changes of morphology in the interphase zone are evidenced in terms of mobility.
Посилання на статтю:
A study of interphase in model composites via low temperature thermo stimulated creep spectroscopy / A. Dufresne* and C. Lacabanne // Polymer. – 1993. – Vol 34. – P. 3173-3178.