A device to obtain the nuclear magnetic resonance (NMR) spectra of poly(2-propenoyl chloride) (PPC) avoiding any contact with the room moisture is described. The 1H and 13C NMR spectra of PPC in THF-d8 solution are thus obtained. The distribution of meso and racemic dyads inferred from the integration of different 1H NMR signals is: (m) 0.45 and (r) 0.55.
Посилання на статтю:
Polymer Communication Characterization of poly(2-propenoyl chloride) by nuclear magnetic resonance spectroscopy / C. Gaillard, M. Camps // Polymer. – 1999. – N 40. – P. 4961–4964.